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How to unlock: You must first have completed up to Level 4: Asylum Assignment in the Story Mode.
Then go to the open world map to look up General Zod, and highlight him on the map using the red exclamation point marker to know where to go. He can be found on a rooftop in the Metro Station (South Island) area of Gotham City.
Defeat him to make him available to buy.
Note: If hitting General Zod doesn’t seem to do any damage, that probably means you’re playing as a normal character. You should keep in mind that on Earth Zod is invincible like all Kryptonians, so you need another invincible character like Superman to defeat him.
Price: 500,000 studs.
Sinestro (Villain)
How to unlock: You must first complete the Story Mode up to Level 4: Asylum Assignment.
Then go to the open world map to look up Sinestro’s location, and highlight him on the map using the red exclamation point marker to know where to go. He can be found on a rooftop in the Metro Station (Central) area of Gotham City.
Defeat him to make him available to buy.
Price: 125,000 studs.